Source code for GSASII.imports.G2phase_CIF

# -*- coding: utf-8 -*-
'''
'''
# Routines to import Phase information from CIF files
from __future__ import division, print_function
import sys
import random as ran
import numpy as np
import re
import copy
import os.path
from .. import GSASIIpath
from .. import GSASIIobj as G2obj
from .. import GSASIIspc as G2spc
from .. import GSASIIElem as G2elem
from .. import GSASIIlattice as G2lat
from .. import GSASIIfiles as G2fil
try:
    import CifFile as cif # PyCifRW from James Hester as a package
except ImportError:
    try:
        from .. import CifFile as cif # PyCifRW, as distributed w/G2 (old)
    except ImportError:
        cif = None
debug = GSASIIpath.GetConfigValue('debug')

# This is a special importer that may use GUI access if it is available.
haveGUI = None  # this is set to True if the GUI is available; False otherwise

#debug = False

[docs] class CIFPhaseReader(G2obj.ImportPhase): 'Implements a phase importer from a possibly multi-block CIF file' def __init__(self): if cif is None: self.UseReader = False msg = 'CIFPhase Reader skipped because PyCifRW (CifFile) module is not installed.' G2fil.ImportErrorMsg(msg,{'CIF Phase importer':['pycifrw']}) print(70*'=') # this needs a special warning print('Warning: you do not have the PyCifRW (CifFile) module installed.') print(' CIF imports not possible. Use the Help/"Add packages..." menu\n command to address') print(70*'=') super(self.__class__,self).__init__( # fancy way to say ImportPhase.__init__ extensionlist=('.CIF','.cif','.mcif'), strictExtension=False, formatName = 'CIF', longFormatName = 'Crystallographic Information File import' ) self.useNet = True # set this to False to prevent access to web (used in scriptable)
[docs] def ContentsValidator(self, filename): fp = open(filename,'r') ok = self.CIFValidator(fp) #print('validator: ',ok) fp.close() return ok
def Reader(self,filename, ParentFrame=None, usedRanIdList=[], **unused): global haveGUI if cif is None: # unexpected, but worth a specific error message print('Attempting to read a CIF without PyCifRW installed') raise Exception('Attempting to read a CIF without PyCifRW installed') isodistort_warnings = '' # errors that would prevent an isodistort analysis self.Phase = G2obj.SetNewPhase(Name='new phase') # create a new empty phase dict # make sure the ranId is really unique! while self.Phase['ranId'] in usedRanIdList: self.Phase['ranId'] = ran.randint(0,sys.maxsize) self.MPhase = G2obj.SetNewPhase(Name='new phase') # create a new empty phase dict # make sure the ranId is really unique! while self.MPhase['ranId'] in usedRanIdList: self.MPhase['ranId'] = ran.randint(0,sys.maxsize) returnstat = False cellitems = ( '_cell_length_a','_cell_length_b','_cell_length_c', '_cell_angle_alpha','_cell_angle_beta','_cell_angle_gamma',) # cellwaveitems = ( # '_cell_wave_vector_seq_id', # '_cell_wave_vector_x','_cell_wave_vector_y','_cell_wave_vector_z') reqitems = ( '_atom_site_fract_x', '_atom_site_fract_y', '_atom_site_fract_z', ) phasenamefields = ( '_chemical_name_common', '_pd_phase_name', '_chemical_formula_sum' ) try: cf = G2obj.ReadCIF(filename) except cif.StarError as msg: msg = f'\nThis file does not have valid CIF syntax. Web site https://checkcif.iucr.org/ can help find CIF errors. If VESTA or https://addie.ornl.gov/conf_viewer is able to read this CIF, it may allow you to rewrite it as a valid file. \n\nError from PyCifRW: {msg}' self.errors = msg self.warnings += msg return False # scan blocks for structural info self.errors = 'Error during scan of blocks for datasets' str_blklist = [] for blk in cf.keys(): for r in reqitems+cellitems: if r not in cf[blk].keys(): break else: str_blklist.append(blk) if not str_blklist: selblk = None # no block to choose elif len(str_blklist) == 1: # only one choice selblk = 0 else: # choose from options choice = [] for blknm in str_blklist: choice.append('') # accumumlate some info about this phase choice[-1] += blknm + ': ' for i in phasenamefields: # get a name for the phase name = cf[blknm].get(i,'phase name').strip() if name is None or name == '?' or name == '.': continue else: choice[-1] += name.strip() + ', ' break na = len(cf[blknm].get("_atom_site_fract_x")) if na == 1: choice[-1] += '1 atom' else: choice[-1] += ('%d' % na) + ' atoms' choice[-1] += ', cell: ' fmt = "%.2f," for i,key in enumerate(cellitems): if i == 3: fmt = "%.f," if i == 5: fmt = "%.f" choice[-1] += fmt % cif.get_number_with_esd( cf[blknm].get(key))[0] sg = cf[blknm].get("_symmetry_space_group_name_H-M",'') if not sg: sg = cf[blknm].get("_space_group_name_H-M_alt",'') if not sg: sg = cf[blknm].get("_space_group_ssg_name",'') if not sg: sg = cf[blknm].get("_space_group.magn_ssg_name_BNS",'') if not sg: sg = cf[blknm].get("_space_group.magn_ssg_name",'') #how about checking for super/magnetic ones as well? - reject 'X'? sg = sg.replace('_','') if sg: choice[-1] += ', (' + sg.strip() + ')' if haveGUI is None: try: import wx from .. import GSASIIctrlGUI as G2G haveGUI = G2G.haveGUI() except: haveGUI = False if haveGUI: selblk = G2G.PhaseSelector(choice,ParentFrame=ParentFrame, title= 'Select a phase from one the CIF data_ blocks below',size=(600,100)) else: print('You are reading a multiblock CIF. Defaulting to the first block') selblk = 0 self.errors = 'Error during reading of selected block' #process selected phase if selblk is None: returnstat = False # no block selected or available else: #do space group symbol & phase type first blknm = str_blklist[selblk] blk = cf[str_blklist[selblk]] E = True Super = False magnetic = False moddim = int(blk.get("_cell_modulation_dimension",'0')) if moddim: #incommensurate if moddim > 1: msg = 'more than 3+1 super symmetry is not allowed in GSAS-II' self.errors = msg self.warnings += '\n'+msg return False if blk.get('_cell_subsystems_number'): msg = 'Composite super structures not allowed in GSAS-II' self.errors = msg self.warnings += '\n'+msg return False sspgrp = blk.get("_space_group_ssg_name",'') if not sspgrp: #might be incommensurate magnetic MSSpGrp = blk.get("_space_group.magn_ssg_name_BNS",'') if not MSSpGrp: MSSpGrp = blk.get("_space_group.magn_ssg_name",'') if not MSSpGrp: msg = 'No incommensurate space group name was found in the CIF.' self.errors = msg self.warnings += '\n'+msg return False if 'X' in MSSpGrp: msg = 'Ad hoc incommensurate magnetic space group '+MSSpGrp+' is not allowed in GSAS-II' self.warnings += '\n'+msg self.errors = msg return False magnetic = True if 'X' in sspgrp: msg = 'Ad hoc incommensurate space group '+sspgrp+' is not allowed in GSAS-II' self.warnings += '\n'+msg self.errors = msg return False Super = True if magnetic: sspgrp = MSSpGrp.split('(') sspgrp[1] = "("+sspgrp[1] SpGrp = G2spc.StandardizeSpcName(sspgrp[0]) if "1'" in SpGrp: sspgrp[1] = sspgrp[1][:-1] #take off extra 's'; gets put back later MSpGrp = sspgrp[0] self.MPhase['General']['Type'] = 'magnetic' self.MPhase['General']['AtomPtrs'] = [3,1,10,12] else: sspgrp = sspgrp.split('(') sspgrp[1] = "("+sspgrp[1] SpGrp = sspgrp[0] if "1'" in SpGrp: #nonmagnetics can't be gray SpGrp = SpGrp.replace("1'",'') sspgrp[1] = sspgrp[1][:-1] #take off extra 's' # SpGrp = G2spc.StandardizeSpcName(SpGrp) self.Phase['General']['Type'] = 'nuclear' if not SpGrp: print (sspgrp) self.warnings += 'Space group name '+sspgrp[0]+sspgrp[1]+' not recognized by GSAS-II' return False SuperSg = sspgrp[1].replace('\\','').replace(',','') SuperVec = [[0,0,.1],False,4] else: #not incommensurate SpGrp = blk.get("_symmetry_space_group_name_H-M",'') if not SpGrp: SpGrp = blk.get("_space_group_name_H-M_alt",'') try: SpGrp = G2spc.spgbyNum[int(blk.get('_symmetry_Int_Tables_number'))] except: pass if SpGrp: SpGrp = SpGrp.replace('_','').split('(')[0] SpGrp = G2spc.fullHM2shortHM(SpGrp) self.Phase['General']['Type'] = 'nuclear' else: #try magnetic MSpGrp = blk.get("_space_group.magn_name_BNS",'') if not MSpGrp: MSpGrp = blk.get("_space_group_magn.name_BNS",'') SpGrp = blk.get('_parent_space_group.name_H-M_alt') if not SpGrp: SpGrp = blk.get('_parent_space_group.name_H-M') if SpGrp and MSpGrp: SpGrp = SpGrp[:2]+SpGrp[2:].replace('_','') #get rid of screw '_' if '_' in SpGrp[1]: SpGrp = SpGrp.split('_')[0]+SpGrp[3:] SpGrp = G2spc.StandardizeSpcName(SpGrp) elif MSpGrp: # have a magnetic sg, but no parent. Look up BNS num. Assume std setting MSpGnum = blk.get("_space_group_magn.number_BNS",'') if MSpGnum: try: SpGrp = G2spc.spgbyNum[int(MSpGnum.split('.')[0])] except: pass if SpGrp: magnetic = True self.MPhase['General']['Type'] = 'magnetic' self.MPhase['General']['AtomPtrs'] = [3,1,10,12] elif MSpGrp: print (f'Magnetic group={MSpGrp} but no parent SG supplied') self.warnings += f'Magnetic group={MSpGrp} but no space group name was found in the CIF.' SpGrp = 'P 1' else: self.warnings += 'No space group name was found in the CIF.' SpGrp = 'P 1' #process space group symbol E,SGData = G2spc.SpcGroup(SpGrp) if E and SpGrp: SpGrpNorm = G2spc.StandardizeSpcName(SpGrp) if SpGrpNorm: E,SGData = G2spc.SpcGroup(SpGrpNorm) # if E: #try lookup from number - found full symbol? # SpGrpNorm = G2spc.spgbyNum[int(blk.get('_symmetry_Int_Tables_number'))] # if SpGrpNorm: # E,SGData = G2spc.SpcGroup(SpGrpNorm) # nope, try the space group "out of the Box" if E: self.warnings += 'ERROR in space group symbol '+SpGrp self.warnings += '\nThe space group has been set to "P 1". ' self.warnings += "Change this in phase's General tab." self.warnings += '\nAre there spaces separating axial fields?\n\nError msg: ' self.warnings += G2spc.SGErrors(E) SGData = G2obj.P1SGData # P 1 self.Phase['General']['SGData'] = SGData # save symmetry operators, if specified (use to check for origin 1 in GSASIIdataGUI OnImportPhase) ops = blk.get("_symmetry_equiv_pos_as_xyz") # try older name 1st if ops: self.SymOps['xyz'] = ops elif blk.get("_space_group_symop_operation_xyz"): self.SymOps['xyz'] = blk.get("_space_group_symop_operation_xyz") else: if 'xyz' in self.SymOps: del self.SymOps['xyz'] if Super: E,SSGData = G2spc.SSpcGroup(SGData,SuperSg) if E: self.warnings += 'Invalid super symmetry symbol '+SpGrp+SuperSg self.warnings += '\n'+E SuperSg = SuperSg[:SuperSg.index(')')+1] self.warnings += '\nNew super symmetry symbol '+SpGrp+SuperSg E,SSGData = G2spc.SSpcGroup(SGData,SuperSg) self.Phase['General']['SSGData'] = SSGData if magnetic: self.MPhase['General']['SGData'] = SGData self.MPhase['General']['SGData']['MagSpGrp'] = MSSpGrp.replace(',','').replace('\\','') self.MPhase['General']['SSGData'] = SSGData if magnetic: #replace std operators with those from cif file - probably not the same! SGData['SGFixed'] = True SGData['SGOps'] = [] SGData['SGCen'] = [] if Super: SSGData['SSGOps'] = [] SSGData['SSGCen'] = [] try: sgoploop = blk.GetLoop('_space_group_symop_magn_ssg_operation.id') sgcenloop = blk.GetLoop('_space_group_symop_magn_ssg_centering.id') opid = sgoploop.GetItemPosition('_space_group_symop_magn_ssg_operation.algebraic')[1] centid = sgcenloop.GetItemPosition('_space_group_symop_magn_ssg_centering.algebraic')[1] except KeyError: #old mag cif names sgoploop = blk.GetLoop('_space_group_symop.magn_ssg_id') sgcenloop = blk.GetLoop('_space_group_symop.magn_ssg_centering_id') opid = sgoploop.GetItemPosition('_space_group_symop.magn_ssg_operation_algebraic')[1] centid = sgcenloop.GetItemPosition('_space_group_symop.magn_ssg_centering_algebraic')[1] spnflp = [] for op in sgoploop: M,T,S = G2spc.MagSSText2MTS(op[opid]) SSGData['SSGOps'].append([np.array(M,dtype=float),T]) SGData['SGOps'].append([np.array(M,dtype=float)[:3,:3],T[:3]]) spnflp.append(S) censpn = [] for cent in sgcenloop: M,C,S = G2spc.MagSSText2MTS(cent[centid]) SSGData['SSGCen'].append(C) SGData['SGCen'].append(C[:3]) censpn += list(np.array(spnflp)*S) self.MPhase['General']['SSGData'] = SSGData else: try: sgoploop = blk.GetLoop('_space_group_symop_magn_operation.id') opid = sgoploop.GetItemPosition('_space_group_symop_magn_operation.xyz')[1] try: sgcenloop = blk.GetLoop('_space_group_symop_magn_centering.id') centid = sgcenloop.GetItemPosition('_space_group_symop_magn_centering.xyz')[1] except KeyError: sgcenloop = None except KeyError: try: sgoploop = blk.GetLoop('_space_group_symop_magn.id') sgcenloop = blk.GetLoop('_space_group_symop_magn_centering.id') opid = sgoploop.GetItemPosition('_space_group_symop_magn_operation.xyz')[1] centid = sgcenloop.GetItemPosition('_space_group_symop_magn_centering.xyz')[1] except KeyError: #old mag cif names sgoploop = blk.GetLoop('_space_group_symop.magn_id') sgcenloop = blk.GetLoop('_space_group_symop.magn_centering_id') opid = sgoploop.GetItemPosition('_space_group_symop.magn_operation_xyz')[1] centid = sgcenloop.GetItemPosition('_space_group_symop.magn_centering_xyz')[1] # generate the SpnFlp and SGspin spin color vectors from mCIF info sgspin = len(SGData['SGSpin'])*[None] opnum = -1 spnflp = [] for op in sgoploop: try: M,T,S = G2spc.MagText2MTS(op[opid]) SGData['SGOps'].append([np.array(M,dtype=float),T]) spnflp.append(S) opnum += 1 sgspin[opnum] = S except KeyError: self.warnings += 'Space group operator '+op[opid]+' is not recognized by GSAS-II' return False censpn = [] if sgcenloop: for i,cent in enumerate(sgcenloop): M,C,S = G2spc.MagText2MTS(cent[centid]) SGData['SGCen'].append(C) censpn += (np.array(spnflp)*S).tolist() if i == 0: continue opnum += 1 sgspin[opnum] = S else: M,C,S = G2spc.MagText2MTS('x,y,z,+1') SGData['SGCen'].append(C) censpn += list(np.array(spnflp)*S) self.MPhase['General']['SGData'] = SGData self.MPhase['General']['SGData']['SpnFlp'] = censpn G2spc.GenMagOps(SGData) #set magMom self.MPhase['General']['SGData']['MagSpGrp'] = MSpGrp if "1'" in MSpGrp: SGData['SGGray'] = True MagPtGp = blk.get('_space_group.magn_point_group') if not MagPtGp: MagPtGp = blk.get('_space_group.magn_point_group_name') if not MagPtGp: MagPtGp = blk.get('_space_group_magn.point_group_name') self.MPhase['General']['SGData']['MagPtGp'] = MagPtGp if None in sgspin: print('Unable to generate all SGspin values') else: SGData['SGSpin'] = sgspin SGData['SGGray'] = not -1 in sgspin # do we have a MagPtGp name and does it have spaces, if not, create it if not MagPtGp or not ' ' in MagPtGp: # generate MagPtGp and fix spacing MagSpGrp SGData['GenSym'] = ['1'] # needed for patch self.MPhase['General']['SGData']['MagSpGrp'] = G2spc.MagSGSym(self.MPhase['General']['SGData']) del SGData['GenSym'] # cell parameters cell = [] for lbl in cellitems: cell.append(cif.get_number_with_esd(blk[lbl])[0]) Volume = G2lat.calc_V(G2lat.cell2A(cell)) self.Phase['General']['Cell'] = [False,]+cell+[Volume,] if magnetic: self.MPhase['General']['Cell'] = [False,]+cell+[Volume,] if Super: waveloop = blk.GetLoop('_cell_wave_vector_seq_id') waveDict = dict(waveloop.items()) SuperVec = [[cif.get_number_with_esd(waveDict['_cell_wave_vector_x'][0].replace('?','0'))[0], cif.get_number_with_esd(waveDict['_cell_wave_vector_y'][0].replace('?','0'))[0], cif.get_number_with_esd(waveDict['_cell_wave_vector_z'][0].replace('?','0'))[0]],False,4] # read in atoms self.errors = 'Error during reading of atoms' atomlbllist = [] # table to look up atom IDs atomloop = blk.GetLoop('_atom_site_label') atomkeys = [i.lower() for i in atomloop.keys()] if not blk.get('_atom_site_type_symbol'): isodistort_warnings += '\natom types are missing. \n Check & revise atom types as needed' if magnetic: try: magmoment = '_atom_site_moment.label' magatomloop = blk.GetLoop(magmoment) magatomkeys = [i.lower() for i in magatomloop.keys()] magatomlabels = blk.get(magmoment) G2MagDict = {'_atom_site_moment.label': 0, '_atom_site_moment.crystalaxis_x':7, '_atom_site_moment.crystalaxis_y':8, '_atom_site_moment.crystalaxis_z':9} except KeyError: magmoment = '_atom_site_moment_label' magatomloop = blk.GetLoop(magmoment) magatomkeys = [i.lower() for i in magatomloop.keys()] magatomlabels = blk.get(magmoment) G2MagDict = {'_atom_site_moment_label': 0, '_atom_site_moment_crystalaxis_x':7, '_atom_site_moment_crystalaxis_y':8, '_atom_site_moment_crystalaxis_z':9} if blk.get('_atom_site_aniso_label'): anisoloop = blk.GetLoop('_atom_site_aniso_label') anisokeys = [i.lower() for i in anisoloop.keys()] anisolabels = blk.get('_atom_site_aniso_label') else: anisoloop = None anisokeys = [] anisolabels = [] if Super: # occFloop = None occCloop = None # occFdict = {} occCdict = {} # displSloop = None displFloop = None MagFloop = None # displSdict = {} displFdict = {} MagFdict = {} UijFloop = None UijFdict = {} #occupancy modulation # if blk.get('_atom_site_occ_Fourier_atom_site_label'): # occFloop = blk.GetLoop('_atom_site_occ_Fourier_atom_site_label') # occFdict = dict(occFloop.items()) if blk.get('_atom_site_occ_special_func_atom_site_label'): #Crenel (i.e. Block Wave) occ occCloop = blk.GetLoop('_atom_site_occ_special_func_atom_site_label') occCdict = dict(occCloop.items()) #position modulation if blk.get('_atom_site_displace_Fourier_atom_site_label'): displFloop = blk.GetLoop('_atom_site_displace_Fourier_atom_site_label') displFdict = dict(displFloop.items()) # if blk.get('_atom_site_displace_special_func_atom_site_label'): #sawtooth # displSloop = blk.GetLoop('_atom_site_displace_special_func_atom_site_label') # displSdict = dict(displSloop.items()) #U modulation if blk.get('_atom_site_U_Fourier_atom_site_label'): UijFloop = blk.GetLoop('_atom_site_U_Fourier_atom_site_label') UijFdict = dict(UijFloop.items()) #Mag moment modulation if blk.get('_atom_site_moment_Fourier_atom_site_label'): MagFloop = blk.GetLoop('_atom_site_moment_Fourier_atom_site_label') MagFdict = dict(MagFloop.items()) Mnames = ['_atom_site_moment_fourier_atom_site_label', '_atom_site_moment_fourier_axis','_atom_site_moment_fourier_wave_vector_seq_id', '_atom_site_moment_fourier_param_sin','_atom_site_moment_fourier_param_cos'] elif blk.get('_atom_site_moment_Fourier.atom_site_label'): MagFloop = blk.GetLoop('_atom_site_moment_Fourier.atom_site_label') MagFdict = dict(MagFloop.items()) Mnames = ['_atom_site_moment_fourier.atom_site_label', '_atom_site_moment_fourier.axis','_atom_site_moment_fourier.wave_vector_seq_id', '_atom_site_moment_fourier_param.sin','_atom_site_moment_fourier_param.cos'] self.Phase['Atoms'] = [] if magnetic: self.MPhase['Atoms'] = [] G2AtomDict = { '_atom_site_type_symbol' : 1, '_atom_site_label' : 0, '_atom_site_fract_x' : 3, '_atom_site_fract_y' : 4, '_atom_site_fract_z' : 5, '_atom_site_occupancy' : 6, '_atom_site_aniso_u_11' : 11, '_atom_site_aniso_u_22' : 12, '_atom_site_aniso_u_33' : 13, '_atom_site_aniso_u_12' : 14, '_atom_site_aniso_u_13' : 15, '_atom_site_aniso_u_23' : 16, } ranIdlookup = {} for aitem in atomloop: atomlist = ['','','',0.,0.,0.,1.0,'',0.,'I',0.01, 0.,0.,0.,0.,0.,0.,] for val,key in zip(aitem,atomkeys): col = G2AtomDict.get(key,-1) if col >= 3: atomlist[col] = cif.get_number_with_esd(val)[0] if col >= 11: atomlist[9] = 'A' # if any Aniso term is defined, set flag elif col is not None and col != -1: atomlist[col] = val elif key in ('_atom_site_thermal_displace_type', '_atom_site_adp_type'): #Iso or Aniso? if val.lower() == 'uani': atomlist[9] = 'A' elif key == '_atom_site_u_iso_or_equiv': uisoval = cif.get_number_with_esd(val)[0] if uisoval is not None: atomlist[10] = uisoval elif key == '_atom_site_b_iso_or_equiv': uisoval = cif.get_number_with_esd(val)[0] if uisoval is not None: atomlist[10] = uisoval/(8*np.pi**2) if not atomlist[1] and atomlist[0]: typ = atomlist[0].rstrip('0123456789-+') if G2elem.CheckElement(typ): atomlist[1] = typ if not atomlist[1]: atomlist[1] = 'Xe' self.warnings += ' Atom type '+typ+' not recognized; Xe assumed\n' if atomlist[0] in anisolabels: # does this atom have aniso values in separate loop? atomlist[9] = 'A' for val,key in zip(anisoloop.GetKeyedPacket('_atom_site_aniso_label',atomlist[0]),anisokeys): col = G2AtomDict.get(key) if col: atomlist[col] = cif.get_number_with_esd(val)[0] if None in atomlist[11:17]: atomlist[9] = 'I' atomlist[11:17] = [0.,0.,0.,0.,0.,0.] atomlist[7],atomlist[8] = G2spc.SytSym(atomlist[3:6],SGData)[:2] atomlist[1] = G2elem.FixValence(atomlist[1]) atomlist.append(ran.randint(0,sys.maxsize)) # add a random Id self.Phase['Atoms'].append(atomlist) ranIdlookup[atomlist[0]] = atomlist[-1] if atomlist[0] in atomlbllist: self.warnings += f' note: repeated atom label: {atomlist[0]}\n' else: atomlbllist.append(atomlist[0]) if magnetic and atomlist[0] in magatomlabels: matomlist = atomlist[:7]+[0.,0.,0.,]+atomlist[7:] for mval,mkey in zip(magatomloop.GetKeyedPacket(magmoment,atomlist[0]),magatomkeys): mcol = G2MagDict.get(mkey,-1) if mcol > 0: matomlist[mcol] = cif.get_number_with_esd(mval)[0] self.MPhase['Atoms'].append(matomlist) if Super: Sfrac = np.zeros((4,2)) Sadp = np.zeros((4,12)) Spos = np.zeros((4,6)) Smag = np.zeros((4,6)) nim = -1 waveType = 'Fourier' if occCdict: for i,item in enumerate(occCdict['_atom_site_occ_special_func_atom_site_label']): if item == atomlist[0]: waveType = 'Crenel' val = occCdict['_atom_site_occ_special_func_crenel_c'][i] Sfrac[0][0] = cif.get_number_with_esd(val)[0] val = occCdict['_atom_site_occ_special_func_crenel_w'][i] Sfrac[0][1] = cif.get_number_with_esd(val)[0] nim = 1 if nim >= 0: Sfrac = [waveType,]+[[sfrac,False] for sfrac in Sfrac[:nim]] else: Sfrac = [] nim = -1 if displFdict: for i,item in enumerate(displFdict['_atom_site_displace_fourier_atom_site_label']): if item == atomlist[0]: waveType = 'Fourier' ix = ['x','y','z'].index(displFdict['_atom_site_displace_fourier_axis'][i]) im = int(displFdict['_atom_site_displace_fourier_wave_vector_seq_id'][i]) if im != nim: nim = im val = displFdict['_atom_site_displace_fourier_param_sin'][i] Spos[im-1][ix] = cif.get_number_with_esd(val)[0] val = displFdict['_atom_site_displace_fourier_param_cos'][i] Spos[im-1][ix+3] = cif.get_number_with_esd(val)[0] if nim >= 0: Spos = [waveType,]+[[spos,False] for spos in Spos[:nim]] else: Spos = [] nim = -1 if UijFdict: nim = -1 for i,item in enumerate(UijFdict['_atom_site_u_fourier_atom_site_label']): if item == atomlist[0]: ix = ['U11','U22','U33','U12','U13','U23'].index(UijFdict['_atom_site_u_fourier_tens_elem'][i]) im = int(UijFdict['_atom_site_u_fourier_wave_vector_seq_id'][i]) if im != nim: nim = im val = UijFdict['_atom_site_u_fourier_param_sin'][i] Sadp[im-1][ix] = cif.get_number_with_esd(val)[0] val = UijFdict['_atom_site_u_fourier_param_cos'][i] Sadp[im-1][ix+6] = cif.get_number_with_esd(val)[0] if nim >= 0: Sadp = ['Fourier',]+[[sadp,False] for sadp in Sadp[:nim]] else: Sadp = [] nim = -1 if MagFdict: nim = -1 for i,item in enumerate(MagFdict[Mnames[0]]): if item == atomlist[0]: ix = ['x','y','z'].index(MagFdict[Mnames[1]][i]) im = int(MagFdict[Mnames[2]][i]) if im != nim: nim = im val = MagFdict[Mnames[3]][i] Smag[im-1][ix] = cif.get_number_with_esd(val)[0] val = MagFdict[Mnames[4]][i] Smag[im-1][ix+3] = cif.get_number_with_esd(val)[0] if nim >= 0: Smag = ['Fourier',]+[[smag,False] for smag in Smag[:nim]] else: Smag = [] SSdict = {'SS1':{'Sfrac':Sfrac,'Spos':Spos,'Sadp':Sadp,'Smag':Smag}} if magnetic and atomlist[0] in magatomlabels: matomlist.append(SSdict) atomlist.append(SSdict) if len(atomlbllist) != len(self.Phase['Atoms']): isodistort_warnings += '\nRepeated atom labels prevents ISODISTORT decode' for lbl in phasenamefields: # get a name for the phase try: name = blk.get(lbl) except: continue if name is None: continue name = name.strip() if name == '?' or name == '.': continue else: break else: # no name found, use block name for lack of a better choice; for isodistort use filename name = blknm if 'isodistort' in name: self.Phase['General']['Name'] = os.path.split(filename)[1].split('.')[0] else: self.Phase['General']['Name'] = name.strip() self.Phase['General']['Super'] = Super self.Phase = copy.deepcopy(self.Phase) #clean copy if magnetic: self.MPhase = copy.deepcopy(self.MPhase) #clean copy self.MPhase['General']['Type'] = 'magnetic' self.MPhase['General']['Name'] = name.strip()+' mag' self.MPhase['General']['Super'] = Super if Super: self.MPhase['General']['Modulated'] = True self.MPhase['General']['SuperVec'] = SuperVec self.MPhase['General']['SuperSg'] = SuperSg if self.MPhase['General']['SGData']['SGGray']: self.MPhase['General']['SuperSg'] += 's' if 'mcif' not in filename: self.Phase = copy.deepcopy(self.MPhase) del self.MPhase else: self.MPhase = None if Super: if self.Phase['General']['SGData']['SGGray']: SGData = self.Phase['General']['SGData'] SGData['SGGray'] = False ncen = len(SGData['SGCen']) SGData['SGCen'] = SGData['SGCen'][:ncen//2] self.Phase['General']['SGData'].update(SGData) self.Phase['General']['Modulated'] = True self.Phase['General']['SuperVec'] = SuperVec self.Phase['General']['SuperSg'] = SuperSg if not self.Phase['General']['SGData']['SGFixed']: self.Phase['General']['SSGData'] = G2spc.SSpcGroup(SGData,SuperSg)[1] if self.ISODISTORT_test(blk): if isodistort_warnings: self.warnings += isodistort_warnings else: self.errors = "Error while processing ISODISTORT constraints" self.ISODISTORT_proc(blk,atomlbllist,ranIdlookup,filename) self.errors = "" returnstat = True if self.SymOps.get('xyz',[]): # did the phase supply symmetry operations? # check if they agree with GSAS-II's setting good = G2spc.CompareSym(self.SymOps['xyz'], SGData=self.Phase['General']['SGData']) if not good: origin2 = False if '-x,-y,-z' in [i.replace(' ','').lower() for i in self.SymOps['xyz']]: origin2 = True # this has center of symmetry at origin so origin1->2 cannot fix this msg = 'This CIF uses a space group setting not compatible with GSAS-II.\n' if self.Phase['General']['SGData']['SpGrp'] in G2spc.spg2origins: msg += '\nThis is likely due to the space group being set in Origin 1 rather than 2.\n' if haveGUI is None: try: import wx from .. import GSASIIctrlGUI as G2G haveGUI = G2G.haveGUI() except: haveGUI = False ans = True if not self.useNet: ans = False print(msg) if origin2: print('\nUnable to correct this, giving up') return False elif haveGUI: msg += ''' Do you want to use Bilbao's "CIF to Standard Setting" web service to transform this into a standard setting? ''' if self.Phase['General']['SGData']['SpGrp'] in G2spc.spg2origins and not origin2: msg += ''' If you say "no" here, a simple origin shift later will be applied as an alternative to the above.''' else: msg += '\nIf you say "no" here you will need to fix this yourself manually.' try: ans = G2G.askQuestion(ParentFrame,msg,'xform structure?') except Exception as err: # fails if non-interactive (no wxPython) print(err) else: print(msg) if ans: print('\nCIF symops do not agree with GSAS-II, calling Bilbao "CIF to Standard Setting" web service.\n') from .. import SUBGROUPS SUBGROUPS.createStdSetting(filename,self) elif not origin2 and self.Phase['General']['SGData']['SpGrp'] in G2spc.spg2origins: print('\nCIF symops do not agree with GSAS-II, applying an origin 1->2 shift.\n') SGData = self.Phase['General']['SGData'] T = G2spc.spg2origins[SGData['SpGrp']] for atom in self.Phase['Atoms']: for i in [0,1,2]: atom[3+i] += T[i] atom[7:9] = G2spc.SytSym(atom[3:6],SGData)[0:2] return returnstat
[docs] def ISODISTORT_test(self,blk): '''Test if there is any ISODISTORT information in CIF At present only _iso_displacivemode..., _iso_occupancymode... and _iso_magneticmode_... are tested. ''' for i in ('_iso_displacivemode_label', '_iso_occupancymode_label', '_iso_magneticmode_label', ): if blk.get(i): return True return False
[docs] def ISODISTORT_proc(self,blk,atomlbllist,ranIdlookup,filename): '''Process ISODISTORT items to create constraints etc. Constraints are generated from information extracted from loops beginning with _iso_ and are placed into self.Constraints, which contains a list of :ref:`constraints tree items <Constraint_definitions_table>` and one dict. The dict contains help text for each generated ISODISTORT variable At present only _iso_displacivemode..., _iso_occupancymode... and _iso_magneticmode... are processed. Not yet processed: _iso_rotationalmode... & _iso_strainmode... ''' def fmtEqn(i,head,l,var,k): 'format a section of a row of variables and multipliers' if np.isclose(k,0): return head,l if len(head) + len(l) > 65: print(head+l) head = 20*' ' l = '' if k < 0 and i > 0: l += ' - ' k = -k elif i > 0: l += ' + ' if k == 1: l += '%s ' % str(var) else: l += '%.3f * %s' % (k,str(var)) return head,l def ISOreadMagModes(): '''Read in the ISODISTORT magnetic modes''' modelist = [] shortmodelist = [] modedispl = [] idlist = [] for id,lbl,val in zip( blk.get('_iso_magneticmode_ID'), blk.get('_iso_magneticmode_label'), blk.get('_iso_magneticmode_value')): idlist.append(int(id)) modelist.append(lbl) modedispl.append(float(val)) ISODISTORT_shortLbl(lbl,shortmodelist) # shorten & make unique # total magnetic moments magVarLbl = [] G2varObj = [] G2magOffset = [] idlist = [] error = False ParentMagVals = {} for lbl,exp in zip( blk.get('_iso_moment_label'), blk.get('_iso_moment_formula') ): if '_' in lbl: albl = lbl[:lbl.rfind('_')] vlbl = lbl[lbl.rfind('_')+1:] else: self.warnings += ' ERROR: _iso_moment_label not parsed: '+lbl error = True continue if vlbl not in ('mx','my','mz') or len(vlbl) != 2: self.warnings += ' ERROR: _iso_moment_label not parsed: '+lbl error = True continue i = 'mxmymz'.index(vlbl)//2 if not ParentMagVals.get(albl): ParentMagVals[albl] = [None,None,None] if '+' in exp: val = exp.split('+')[0].strip() val = G2fil.FormulaEval(val) elif '-' in exp: # BHT: how will the offset be subtracted rather than added? val = exp.split('-')[0].strip() val = G2fil.FormulaEval(val) else: val = G2fil.FormulaEval(exp) if val is None: self.warnings += ' ERROR: _iso_moment_formula not interpreted: '+lbl error = True continue else: ParentMagVals[albl][i] = val if val != 0: print(f'Warning moment offset for {albl} is non-zero.\nThis is probably not handled correctly') if error: print (self.warnings) raise Exception("Error decoding variable labels") error = False magIsoNam = {xyz:i for i,xyz in enumerate(('dmx','dmy','dmz'))} for id,lbl,val in zip( blk.get('_iso_deltamoment_ID'), blk.get('_iso_deltamoment_label'), blk.get('_iso_deltamoment_value') ): idlist.append(int(id)) magVarLbl.append(lbl) if '_' in lbl: albl = lbl[:lbl.rfind('_')] vlbl = lbl[lbl.rfind('_')+1:] else: self.warnings += ' ERROR: _iso_deltamoment_label not parsed: '+lbl error = True continue if albl not in atomlbllist: self.warnings += ' ERROR: _iso_deltamoment_label atom not found: '+lbl error = True continue var = varLookup.get(vlbl) if not var: self.warnings += ' ERROR: _iso_deltamoment_label variable not found: '+lbl error = True continue G2magOffset.append(ParentMagVals[albl][magIsoNam[vlbl]] - float(val)) G2varObj.append(G2obj.G2VarObj( (self.Phase['ranId'],None,var,ranIdlookup[albl]) )) if error: raise Exception("Error decoding variable labels") # just in case the items are not ordered increasing by id, sort them here magVarLbl = [i for i,j in sorted(zip(magVarLbl,idlist),key=lambda k:k[1])] G2varObj = [i for i,j in sorted(zip(G2varObj,idlist),key=lambda k:k[1])] if len(G2varObj) != len(modelist): print ("non-square input") raise Exception("Rank of _iso_magneticmode != _iso_deltamoment") # normalization constants normlist = [] idlist = [] for id,exp in zip( blk.get('_iso_magneticmodenorm_ID'), blk.get('_iso_magneticmodenorm_value'), ): idlist.append(int(id)) normlist.append(float(exp)) normlist = [i for i,j in sorted(zip(normlist,idlist),key=lambda k:k[1])] # get mapping of modes to magnetic moments magneticmodematrix = np.zeros((len(G2varObj),len(G2varObj))) for row,col,val in zip( blk.get('_iso_magneticmodematrix_row'), blk.get('_iso_magneticmodematrix_col'), blk.get('_iso_magneticmodematrix_value'),): magneticmodematrix[int(row)-1,int(col)-1] = float(val) # Invert to get mapping of atom displacements to modes Var2ModeMatrix = np.linalg.inv(magneticmodematrix) # create the constraints modeVarList = [] for i,(row,norm) in enumerate(zip(Var2ModeMatrix,normlist)): constraint = [] for j,(lbl,k) in enumerate(zip(magVarLbl,row)): if k == 0: continue constraint.append([k/norm,G2varObj[j]]) modeVar = G2obj.G2VarObj( (self.Phase['ranId'],None,shortmodelist[i],None)) modeVarList.append(modeVar) constraint += [modeVar,False,'f'] self.Constraints.append(constraint) # get the ISODISTORT unit cell xform info #orig_cell = [] #for i in ('_iso_parentcell_length_a','_iso_parentcell_length_b','_iso_parentcell_length_c', # '_iso_parentcell_angle_alpha','_iso_parentcell_angle_beta','_iso_parentcell_angle_gamma'): # orig_cell.append(cif.get_number_with_esd(blk[i])[0]) # save the ISODISTORT info for magnetic mode analysis if 'ISODISTORT' not in self.Phase: self.Phase['ISODISTORT'] = {} self.Phase['ISODISTORT'].update({ # magnetic moment items 'MagVarList' : magVarLbl, 'G2VarList' : G2varObj, 'BaseMag' : G2magOffset, # mode items 'MagModeList' : modelist, 'G2MagModeList' : modeVarList, 'NormList' : normlist, # transform matrices 'Var2ModeMatrix' : Var2ModeMatrix, 'Mode2VarMatrix' : magneticmodematrix, }) # is there ISODISTORT parent->mag cell x-formation info here? xformstr = blk.get('_iso_parent-to-child.transform_Pp_abc') if xformstr: # Make entry that will be used in OnImportPhase (GSASIIdataGUI) # to generate constraints to parent phase mtrx,vec = parse_parent2mag(xformstr) self.Phase['ISODISTORT']['XformInfo'] = {'Trans':mtrx,'offset':vec} explainMode(modelist,shortmodelist) # make explanation dictionary #=== Debug: regenerate input ======================================= if debug: print('\n' + 70*'=') print('ISO modes from Iso coordinate vars (using Var2ModeMatrix, IsoVarList, G2VarList & G2ModeList)' ) for i,row in enumerate(self.Phase['ISODISTORT']['Var2ModeMatrix']): norm = self.Phase['ISODISTORT']['NormList'][i] head = ' ' + str(self.Phase['ISODISTORT']['G2MagModeList'][i]) + ' = (' line = '' for j,(lbl,k) in enumerate(zip(magVarLbl,row)): var = self.Phase['ISODISTORT']['MagVarList'][j] head,line = fmtEqn(j,head,line,var,k) print(head+line+') / {:.3g}'.format(norm)) head = ' = ' line = '' for j,(lbl,k) in enumerate(zip(magVarLbl,row)): var = self.Phase['ISODISTORT']['MagVarList'][j] head,line = fmtEqn(j,head,line,var,k/norm) print(head+line) print('\nConstraints') for c in self.Constraints: if type(c) is dict: continue if c[-1] != 'f': continue line = '' head = ' ' + str(c[-3]) + ' = ' for j,(k,var) in enumerate(c[:-3]): head,line = fmtEqn(j,head,line,var,k) print(head+line) # Get the ISODISTORT offset values coordVarDelta = {} for lbl,val in zip( blk.get('_iso_deltamoment_label'), blk.get('_iso_deltamoment_value'),): coordVarDelta[lbl] = float(val) modeVarDelta = {} for lbl,val in zip( blk.get('_iso_magneticmode_label'), blk.get('_iso_magneticmode_value'),): modeVarDelta[lbl] = cif.get_number_with_esd(val)[0] print('\n' + 70*'=') print('Confirming inverse mode relations computed from displacement values', '\nusing Var2ModeMatrix, NormList, MagVarList') # compute the mode values from the reported coordinate deltas for i,(row,n) in enumerate(zip(self.Phase['ISODISTORT']['Var2ModeMatrix'], self.Phase['ISODISTORT']['NormList'])): line = '' print(str(self.Phase['ISODISTORT']['MagModeList'][i])+' = ') head = ' = (' for j,(lbl,k) in enumerate(zip(magVarLbl,row)): head,line = fmtEqn(j,head,line,lbl,k) print(head+line+') / '+('%.3f'%n)) line = '' head = ' = (' vsum = 0. for j,(lbl,k) in enumerate(zip(magVarLbl,row)): val = "{:3g}".format(coordVarDelta[lbl]) head,line = fmtEqn(j,head,line,val,k) vsum += coordVarDelta[lbl] * k print(head+line+') / '+('%.3f'%n)) fileval = modeVarDelta[self.Phase['ISODISTORT']['MagModeList'][i]] print("{} = {:4g} (value read from CIF = {:4g})\n".format( self.Phase['ISODISTORT']['MagModeList'][i], vsum, fileval)) print( 70*'=') print('Direct displacement relations computed from ISO modes in CIF', '\nusing Mode2VarMatrix, NormList, MagModeList, IsoVarList',) # compute the coordinate displacements from the reported mode values for lbl,row in zip(self.Phase['ISODISTORT']['MagVarList'], self.Phase['ISODISTORT']['Mode2VarMatrix']): l = '' s = 0.0 head = lbl+' =' for j,(k,n) in enumerate(zip(row,self.Phase['ISODISTORT']['NormList'])): if k == 0: continue if len(l) > 65: print(head,l) head = 20*' ' l = '' l1 = '' k1 = k if j > 0 and k < 0: k1 = -k l1 = ' - ' elif j > 0: l1 += ' + ' l += '{:} {:3g} * {:4g} * {:}'.format( l1, k1, n, self.Phase['ISODISTORT']['MagModeList'][j]) s += n * modeVarDelta[self.Phase['ISODISTORT']['MagModeList'][j]] * k print(head,l) print(lbl,'=',s) print(lbl,'==>',str(self.Phase['ISODISTORT']['G2VarList'][i]),'\n') DeltaCoords = {} for i,lbl,row in zip(range(len(magVarLbl)),magVarLbl,magneticmodematrix): s = 0.0 for j,(k,n) in enumerate(zip(row,self.Phase['ISODISTORT']['NormList'])): s += k * n * modeVarDelta[self.Phase['ISODISTORT']['MagModeList'][j]] at,d = lbl.rsplit('_',1) if at not in DeltaCoords: DeltaCoords[at] = [0,0,0] if d == 'dx': DeltaCoords[at][0] = s elif d == 'dy': DeltaCoords[at][1] = s elif d == 'dz': DeltaCoords[at][2] = s #else: # print('unexpected',d) print( 70*'=') print('Moment checks') print("\nMoments computed from ISO mode values, as above") for at in sorted(DeltaCoords): s = at for i in range(3): s += ' ' s += str(ParentMagVals[at][i]+DeltaCoords[at][i]) print(s) # determine the coordinate delta values from deviations from the parent structure print("\nMoment values read directly from CIF") for lbl,mx,my,mz in zip( blk.get('_atom_site_moment.label'), blk.get('_atom_site_moment.crystalaxis_x'), blk.get('_atom_site_moment.crystalaxis_y'), blk.get('_atom_site_moment.crystalaxis_z'), ): print( lbl,mx,my,mz) print('\n' + 70*'=') print("G2 short name ==> ISODISTORT full name", " (from MagModeList and G2MagModeList)") for mode,G2mode in zip(self.Phase['ISODISTORT']['MagModeList'], self.Phase['ISODISTORT']['G2MagModeList']): print('{} ==> {}'.format(str(G2mode), mode)) print('\nConstraint help dict info') for i in self.Constraints: if type(i) is dict: for key in i: print('\t',key,':',i[key]) print( 70*'=') def ISOreadDisplModes(): '''Read in the ISODISTORT displacement modes''' modelist = [] shortmodelist = [] modedispl = [] idlist = [] for id,lbl,val in zip( blk.get('_iso_displacivemode_ID'), blk.get('_iso_displacivemode_label'), blk.get('_iso_displacivemode_value')): idlist.append(int(id)) modelist.append(lbl) modedispl.append(float(val)) ISODISTORT_shortLbl(lbl,shortmodelist) # shorten & make unique # just in case the items are not ordered increasing by id, sort them here modelist = [i for i,j in sorted(zip(modelist,idlist),key=lambda k:k[1])] shortmodelist = [i for i,j in sorted(zip(shortmodelist,idlist),key=lambda k:k[1])] # read in the coordinate offset variables names and map them to G2 names/objects coordVarLbl = [] G2varObj = [] G2coordOffset = [] idlist = [] error = False ParentCoordinates = {} for lbl,exp in zip( blk.get('_iso_coordinate_label'), blk.get('_iso_coordinate_formula') ): if '_' in lbl: albl = lbl[:lbl.rfind('_')] vlbl = lbl[lbl.rfind('_')+1:] else: self.warnings += ' ERROR: _iso_coordinate_label not parsed: '+lbl error = True continue if vlbl not in 'xyz' or len(vlbl) != 1: self.warnings += ' ERROR: _iso_coordinate_label coordinate not parsed: '+lbl error = True continue i = 'xyz'.index(vlbl) if not ParentCoordinates.get(albl): ParentCoordinates[albl] = [None,None,None] if '+' in exp: val = exp.split('+')[0].strip() val = G2fil.FormulaEval(val) elif '-' in exp: val = exp.split('-')[0].strip() val = G2fil.FormulaEval(val) else: val = G2fil.FormulaEval(exp) if val is None: self.warnings += ' ERROR: _iso_coordinate_formula coordinate not interpreted: '+lbl error = True continue else: ParentCoordinates[albl][i] = val if error: print (self.warnings) raise Exception("Error decoding variable labels") error = False coordOffset = {xyz:i for i,xyz in enumerate(('dx','dy','dz'))} for id,lbl,val in zip( blk.get('_iso_deltacoordinate_ID'), blk.get('_iso_deltacoordinate_label'), blk.get('_iso_deltacoordinate_value') ): idlist.append(int(id)) coordVarLbl.append(lbl) if '_' in lbl: albl = lbl[:lbl.rfind('_')] vlbl = lbl[lbl.rfind('_')+1:] else: self.warnings += ' ERROR: _iso_deltacoordinate_label not parsed: '+lbl error = True continue if albl not in atomlbllist: self.warnings += ' ERROR: _iso_deltacoordinate_label atom not found: '+lbl error = True continue var = varLookup.get(vlbl) if not var: self.warnings += ' ERROR: _iso_deltacoordinate_label variable not found: '+lbl error = True continue G2coordOffset.append(ParentCoordinates[albl][coordOffset[vlbl]] - float(val)) G2varObj.append(G2obj.G2VarObj( (self.Phase['ranId'],None,var,ranIdlookup[albl]) )) if error: raise Exception("Error decoding variable labels") # just in case the items are not ordered increasing by id, sort them here coordVarLbl = [i for i,j in sorted(zip(coordVarLbl,idlist),key=lambda k:k[1])] G2varObj = [i for i,j in sorted(zip(G2varObj,idlist),key=lambda k:k[1])] if len(G2varObj) != len(modelist): print ("non-square input") raise Exception("Rank of _iso_displacivemode != _iso_deltacoordinate") # normalization constants normlist = [] idlist = [] for id,exp in zip( blk.get('_iso_displacivemodenorm_ID'), blk.get('_iso_displacivemodenorm_value'), ): idlist.append(int(id)) normlist.append(float(exp)) normlist = [i for i,j in sorted(zip(normlist,idlist),key=lambda k:k[1])] # get mapping of modes to atomic coordinate displacements displacivemodematrix = np.zeros((len(G2varObj),len(G2varObj))) for row,col,val in zip( blk.get('_iso_displacivemodematrix_row'), blk.get('_iso_displacivemodematrix_col'), blk.get('_iso_displacivemodematrix_value'),): displacivemodematrix[int(row)-1,int(col)-1] = float(val) # Invert to get mapping of atom displacements to modes Var2ModeMatrix = np.linalg.inv(displacivemodematrix) # create the constraints modeVarList = [] for i,(row,norm) in enumerate(zip(Var2ModeMatrix,normlist)): constraint = [] for j,(lbl,k) in enumerate(zip(coordVarLbl,row)): if k == 0: continue constraint.append([k/norm,G2varObj[j]]) modeVar = G2obj.G2VarObj( (self.Phase['ranId'],None,shortmodelist[i],None)) modeVarList.append(modeVar) constraint += [modeVar,False,'f'] self.Constraints.append(constraint) #---------------------------------------------------------------------- # save the ISODISTORT info for displacive mode analysis if 'ISODISTORT' not in self.Phase: self.Phase['ISODISTORT'] = {} self.Phase['ISODISTORT'].update({ # coordinate items 'IsoVarList' : coordVarLbl, 'G2VarList' : G2varObj, 'G2coordOffset' : G2coordOffset, 'G2parentCoords' : [ParentCoordinates[item] for item in ParentCoordinates], #Assumes python 3.7 dict ordering! # mode items 'IsoModeList' : modelist, 'G2ModeList' : modeVarList, 'NormList' : normlist, 'modeDispl' : modedispl, 'ISOmodeDispl' : copy.deepcopy(modedispl), # transform matrices 'Var2ModeMatrix' : Var2ModeMatrix, 'Mode2VarMatrix' : displacivemodematrix, }) explainMode(modelist,shortmodelist) # make explanation dictionary #=== Debug: regenerate input ======================================= if debug: print('\n' + 70*'=') print('ISO modes from Iso coordinate vars (using Var2ModeMatrix, IsoVarList, G2VarList & G2ModeList)' ) for i,row in enumerate(self.Phase['ISODISTORT']['Var2ModeMatrix']): norm = self.Phase['ISODISTORT']['NormList'][i] head = ' ' + str(self.Phase['ISODISTORT']['G2ModeList'][i]) + ' = (' line = '' for j,(lbl,k) in enumerate(zip(coordVarLbl,row)): var = self.Phase['ISODISTORT']['IsoVarList'][j] head,line = fmtEqn(j,head,line,var,k) print(head+line+') / {:.3g}'.format(norm)) head = ' = ' line = '' for j,(lbl,k) in enumerate(zip(coordVarLbl,row)): var = self.Phase['ISODISTORT']['IsoVarList'][j] head,line = fmtEqn(j,head,line,var,k/norm) print(head+line) print('\nConstraints') for c in self.Constraints: if type(c) is dict: continue if c[-1] != 'f': continue line = '' head = ' ' + str(c[-3]) + ' = ' for j,(k,var) in enumerate(c[:-3]): head,line = fmtEqn(j,head,line,var,k) print(head+line) # Get the ISODISTORT offset values coordVarDelta = {} for lbl,val in zip( blk.get('_iso_deltacoordinate_label'), blk.get('_iso_deltacoordinate_value'),): coordVarDelta[lbl] = float(val) modeVarDelta = {} for lbl,val in zip( blk.get('_iso_displacivemode_label'), blk.get('_iso_displacivemode_value'),): modeVarDelta[lbl] = cif.get_number_with_esd(val)[0] print('\n' + 70*'=') print('Confirming inverse mode relations computed from displacement values', '\nusing Var2ModeMatrix, NormList, IsoVarList') # compute the mode values from the reported coordinate deltas for i,(row,n) in enumerate(zip(self.Phase['ISODISTORT']['Var2ModeMatrix'], self.Phase['ISODISTORT']['NormList'])): line = '' print(str(self.Phase['ISODISTORT']['IsoModeList'][i])+' = ') head = ' = (' for j,(lbl,k) in enumerate(zip(coordVarLbl,row)): head,line = fmtEqn(j,head,line,lbl,k) print(head+line+') / '+('%.3f'%n)) line = '' head = ' = (' vsum = 0. for j,(lbl,k) in enumerate(zip(coordVarLbl,row)): val = "{:3g}".format(coordVarDelta[lbl]) head,line = fmtEqn(j,head,line,val,k) vsum += coordVarDelta[lbl] * k print(head+line+') / '+('%.3f'%n)) fileval = modeVarDelta[self.Phase['ISODISTORT']['IsoModeList'][i]] print("{} = {:4g} (value read from CIF = {:4g})\n".format( self.Phase['ISODISTORT']['IsoModeList'][i], vsum, fileval)) print( 70*'=') print('Direct displacement relations computed from ISO modes in CIF', '\nusing Mode2VarMatrix, NormList, IsoModeList, IsoVarList',) # compute the coordinate displacements from the reported mode values for lbl,row in zip(self.Phase['ISODISTORT']['IsoVarList'], self.Phase['ISODISTORT']['Mode2VarMatrix']): l = '' s = 0.0 head = lbl+' =' for j,(k,n) in enumerate(zip(row,self.Phase['ISODISTORT']['NormList'])): if k == 0: continue if len(l) > 65: print(head,l) head = 20*' ' l = '' l1 = '' k1 = k if j > 0 and k < 0: k1 = -k l1 = ' - ' elif j > 0: l1 += ' + ' l += '{:} {:3g} * {:4g} * {:}'.format( l1, k1, n, self.Phase['ISODISTORT']['IsoModeList'][j]) s += n * modeVarDelta[self.Phase['ISODISTORT']['IsoModeList'][j]] * k print(head,l) print(lbl,'=',s) print(lbl,'==>',str(self.Phase['ISODISTORT']['G2VarList'][i]),'\n') DeltaCoords = {} for i,lbl,row in zip(range(len(coordVarLbl)),coordVarLbl,displacivemodematrix): s = 0.0 for j,(k,n) in enumerate(zip(row,self.Phase['ISODISTORT']['NormList'])): s += k * n * modeVarDelta[self.Phase['ISODISTORT']['IsoModeList'][j]] at,d = lbl.rsplit('_',1) if at not in DeltaCoords: DeltaCoords[at] = [0,0,0] if d == 'dx': DeltaCoords[at][0] = s elif d == 'dy': DeltaCoords[at][1] = s elif d == 'dz': DeltaCoords[at][2] = s #else: # print('unexpected',d) print( 70*'=') print('Coordinate checks') print("\nxyz's Computed from ISO mode values, as above") for at in sorted(DeltaCoords): s = at for i in range(3): s += ' ' s += str(ParentCoordinates[at][i]+DeltaCoords[at][i]) print(s) # determine the coordinate delta values from deviations from the parent structure print("\nxyz Values read directly from CIF") for atmline in self.Phase['Atoms']: lbl = atmline[0] x,y,z = atmline[3:6] print( lbl,x,y,z) print('\n' + 70*'=') print("G2 short name ==> ISODISTORT full name", " (from IsoModeList and G2ModeList)") for mode,G2mode in zip(self.Phase['ISODISTORT']['IsoModeList'], self.Phase['ISODISTORT']['G2ModeList']): print('{} ==> {}'.format(str(G2mode), mode)) print('\nConstraint help dict info') for i in self.Constraints: if type(i) is dict: for key in i: print('\t',key,':',i[key]) print( 70*'=') def ISOreadOccModes(): '''Read in the ISODISTORT occupancy modes''' modelist = [] shortmodelist = [] idlist = [] for id,lbl in zip( blk.get('_iso_occupancymode_ID'), blk.get('_iso_occupancymode_label')): idlist.append(int(id)) modelist.append(lbl) ISODISTORT_shortLbl(lbl,shortmodelist) # shorten & make unique # just in case the items are not ordered increasing by id, sort them here modelist = [i for i,j in sorted(zip(modelist,idlist),key=lambda k:k[1])] shortmodelist = [i for i,j in sorted(zip(shortmodelist,idlist),key=lambda k:k[1])] # read in the coordinate offset variables names and map them to G2 names/objects occVarLbl = [] G2varObj = [] idlist = [] error = False for id,lbl in zip( blk.get('_iso_deltaoccupancy_ID'), blk.get('_iso_deltaoccupancy_label') ): idlist.append(int(id)) occVarLbl.append(lbl) if '_' in lbl: albl = lbl[:lbl.rfind('_')] vlbl = lbl[lbl.rfind('_')+1:] else: self.warnings += ' ERROR: _iso_deltaoccupancy_label not parsed: '+lbl error = True continue if albl not in atomlbllist: self.warnings += ' ERROR: _iso_deltaoccupancy_label atom not found: '+lbl error = True continue var = varLookup.get(vlbl) if not var: self.warnings += ' ERROR: _iso_deltaoccupancy_label variable not found: '+lbl error = True continue G2varObj.append(G2obj.G2VarObj( (self.Phase['ranId'],None,var,ranIdlookup[albl]) )) if error: raise Exception("Error decoding variable labels") # just in case the items are not ordered increasing by id, sort them here occVarLbl = [i for i,j in sorted(zip(occVarLbl,idlist),key=lambda k:k[1])] G2varObj = [i for i,j in sorted(zip(G2varObj,idlist),key=lambda k:k[1])] if len(G2varObj) != len(modelist): print ("non-square input") raise Exception("Rank of _iso_occupancymode != _iso_deltaoccupancy") error = False ParentOcc = {} for lbl,exp in zip( blk.get('_iso_occupancy_label'), blk.get('_iso_occupancy_formula') ): if '_' in lbl: albl = lbl[:lbl.rfind('_')] vlbl = lbl[lbl.rfind('_')+1:] else: self.warnings += ' ERROR: _iso_occupancy_label not parsed: '+lbl error = True continue if vlbl != 'occ': self.warnings += ' ERROR: _iso_occupancy_label coordinate not parsed: '+lbl error = True continue if '+' in exp: val = exp.split('+')[0].strip() val = G2fil.FormulaEval(val) if val is None: self.warnings += ' ERROR: _iso_occupancy_formula coordinate not interpreted: '+lbl error = True continue ParentOcc[albl] = val if error: raise Exception("Error decoding occupancy labels") # get mapping of modes to atomic coordinate displacements occupancymodematrix = np.zeros((len(G2varObj),len(G2varObj))) for row,col,val in zip( blk.get('_iso_occupancymodematrix_row'), blk.get('_iso_occupancymodematrix_col'), blk.get('_iso_occupancymodematrix_value'),): occupancymodematrix[int(row)-1,int(col)-1] = float(val) # Invert to get mapping of atom displacements to modes occupancymodeInvmatrix = np.linalg.inv(occupancymodematrix) # create the constraints modeVarList = [] for i,row in enumerate(occupancymodeInvmatrix): constraint = [] for j,(lbl,k) in enumerate(zip(occVarLbl,row)): if k == 0: continue constraint.append([k,G2varObj[j]]) modeVar = G2obj.G2VarObj( (self.Phase['ranId'],None,shortmodelist[i],None)) modeVarList.append(modeVar) constraint += [modeVar,False,'f'] self.Constraints.append(constraint) # normilization constants normlist = [] idlist = [] for id,exp in zip( blk.get('_iso_occupancymodenorm_ID'), blk.get('_iso_occupancymodenorm_value'), ): idlist.append(int(id)) normlist.append(float(exp)) normlist = [i for i,j in sorted(zip(normlist,idlist),key=lambda k:k[1])] #---------------------------------------------------------------------- # save the ISODISTORT info for occupancy mode analysis if 'ISODISTORT' not in self.Phase: self.Phase['ISODISTORT'] = {} self.Phase['ISODISTORT'].update({ # coordinate items 'OccVarList' : occVarLbl, 'G2OccVarList' : G2varObj, 'BaseOcc' : ParentOcc, # mode items 'OccModeList' : modelist, 'G2OccModeList' : modeVarList, 'OccNormList' : normlist, # transform matrices 'Var2OccMatrix' : occupancymodeInvmatrix, 'Occ2VarMatrix' : occupancymodematrix, }) explainMode(modelist,shortmodelist) # make explanation dictionary #=== Debug: regenerate input ======================================= if debug: # coordinate items G2varObj = self.Phase['ISODISTORT']['G2OccVarList'] # mode items modelist = self.Phase['ISODISTORT']['OccModeList'] modeVarList = self.Phase['ISODISTORT']['G2OccModeList'] normlist = self.Phase['ISODISTORT']['OccNormList'] print('\n' + 70*'=') print( 70*'=') print('\nVar2OccMatrix' ,'OccVarList' ) for i,row in enumerate(occupancymodeInvmatrix): l = '' for j,(lbl,k) in enumerate(zip(occVarLbl,row)): if k == 0: continue if l: l += ' + ' #l += lbl+' * '+str(k) l += str(G2varObj[j])+' * '+str(k) print( str(i) + ': '+str(modeVarList[i])+' = '+l) # Get the ISODISTORT offset values occVarDelta = {} for lbl,val in zip( blk.get('_iso_deltaoccupancy_label'), blk.get('_iso_deltaoccupancy_value'),): occVarDelta[lbl] = float(val) modeVarDelta = {} for lbl,val in zip( blk.get('_iso_occupancymode_label'), blk.get('_iso_occupancymode_value'),): modeVarDelta[lbl] = cif.get_number_with_esd(val)[0] print( 70*'=') print('\nInverse relations using Var2OccModeMatrix, OccNormList, OccVarList') # compute the mode values from the reported coordinate deltas for i,(row,n) in enumerate(zip(occupancymodeInvmatrix,normlist)): l = '' for lbl,k in zip(occVarLbl,row): if k == 0: continue if l: l += ' + ' l += lbl+' * '+str(k) print('a'+str(i)+' = '+str(modeVarList[i])+' = ('+l+')/'+str(n)) print('\nCalculation checks\n') for i,(row,n) in enumerate(zip(occupancymodeInvmatrix,normlist)): #l = '' sl = '' s = 0. for lbl,k in zip(occVarLbl,row): if k == 0: continue #if l: l += ' + ' #l += lbl+' * '+str(k) if sl: sl += ' + ' sl += str(occVarDelta[lbl])+' * '+str(k) s += occVarDelta[lbl] * k print(str(modeVarList[i]),'=','('+sl+') / ',n,'=',s/n) print(' ?= ',modeVarDelta[modelist[i]]) print() print( 70*'=') print('\nDirect relations using Occ2VarMatrix, OccNormList, OccVarList') # compute the coordinate displacements from the reported mode values Occ = {} for i,lbl,row in zip(range(len(occVarLbl)),occVarLbl,occupancymodematrix): l = '' s = 0.0 for j,(k,n) in enumerate(zip(row,normlist)): if k == 0: continue if l: l += ' + ' l += str(n)+' * '+str(modeVarList[j])+' * '+str(k) s += n * modeVarDelta[modelist[j]] * k print( lbl,'=',str(G2varObj[i]),'=',l,'=',s,'\n') j = lbl.split('_')[0] Occ[j] = ParentOcc[j]+s # determine the coordinate delta values from deviations from the parent structure print('\nOccupancy from CIF vs computed') for atmline in self.Phase['Atoms']: lbl = atmline[0] if lbl in Occ: print( lbl,atmline[6],Occ[lbl]) print( 70*'=') print('\nGenerated constraints') for i in self.Constraints: if type(i) is dict: print('\nconstraint help dict') for key in i: print('\t',key,':',i[key]) elif i[-1] == 'f': print('\n\t',i[-3],' =') for m,j in i[:-3]: print('\t\t+',m,' * ',j,' ',repr(j)) else: print(' unexpected: ',repr(i)) print("\nG2name ==> ISODISTORT full name", ".Phase['ISODISTORT']['OccModeList']", ".Phase['ISODISTORT']['G2OccModeList']") for mode,G2mode in zip(modelist,modeVarList): print(" ?::"+str(G2mode),' ==>', mode) def explainMode(modelist,shortmodelist): explanation = {} for mode,shortmode in zip(modelist,shortmodelist): modeVar = G2obj.G2VarObj( (self.Phase['ranId'],None,shortmode,None)) explanation[modeVar] = ("Full ISODISTORT name for " + shortmode + " is " + str(mode)) if explanation: self.Constraints.append(explanation) #### code for ISODISTORT_proc starts here------------------------------ varLookup = {'dx':'dAx','dy':'dAy','dz':'dAz','do':'Afrac', 'dmx':'AMx', 'dmy':'AMy', 'dmz':'AMz'} 'Maps ISODISTORT parm names to GSAS-II names' # used for all types of modes self.Constraints = [] G2obj.AddPhase2Index(self,filename) # put phase info into Var index #---------------------------------------------------------------------- if blk.get('_iso_displacivemode_label'): # Read in the ISODISTORT displacement modes here ISOreadDisplModes() elif blk.get('_iso_occupancymode_label'): # Read in the ISODISTORT occupancy modes here ISOreadOccModes() elif blk.get('_iso_magneticmode_label'): # Read in the ISODISTORT magnetic modes here ISOreadMagModes()
[docs] def ISODISTORT_shortLbl(lbl,shortmodelist): '''Shorten model labels and remove special characters ''' regexp = re.match(r'.*?\[.*?\](.*?)\(.*?\)\[.*?\](.*)',lbl) # assume lbl is of form SSSSS[x,y,z]AAAA(a,b,...)[...]BBBBB # where SSSSS is the parent spacegroup, [x,y,z] is a location, etc. if regexp: # this extracts the AAAAA and BBBBB parts of the string lbl = regexp.expand(r'\1\2') # parse succeeded, make a short version else: # try form SSSSS[x,y,z]AAAA(a,b,...)BBBBB regexp = re.match(r'.*?\[.*?\](.*?)\(.*?\)(.*)',lbl) if regexp: lbl = regexp.expand(r'\1\2') # parse succeeded, make a short version lbl = lbl.replace('order','o') lbl = lbl.replace('+','_') lbl = lbl.replace('-','_') G2obj.MakeUniqueLabel(lbl,shortmodelist) # make unique and add to list
[docs] def parse_parent2mag(s): '''Parse _iso_parent-to-child.transform_Pp_abc with strings like: 'a,-b,-c;0.5,0,0' 'a+b,-a+b,c;0,0,0' into: (matrix, vector) Returns: matrix: list[list[int]] vector: list[float]] ''' import re def parse_expr(expr): expr = expr.replace(" ", "") if not expr: raise ValueError("Empty expression") coeffs = {"a":0, "b":0, "c":0} # normalize so every term has explicit sign if expr[0] not in "+-": expr = "+" + expr # split into signed terms like +a, -b, +2a, -3c terms = re.findall(r"[+-][^+-]+", expr) for term in terms: sign = -1 if term[0] == "-" else 1 body = term[1:] m = re.fullmatch(r"(\d+)?([A-Za-z]+)", body) if not m: raise ValueError(f"Unsupported term: {term}") n, var = m.groups() if var not in coeffs: raise ValueError(f"Unknown variable: {var}") coeff = int(n) if n else 1 coeffs[var] += sign * coeff return [coeffs[v] for v in ("a", "b", "c")] if ";" in s: expr_part, vec_part = s.split(";", 1) else: expr_part, vec_part = s, "0,0,0" exprs = [x.strip() for x in expr_part.split(",")] if len(exprs) != 3: raise ValueError(f"Expected 3 expressions, got {len(exprs)}") vec = [float(x.strip()) for x in vec_part.split(",")] if len(vec) != 3: raise ValueError(f"Expected 3 vector entries, got {len(vec)}") matrix = [parse_expr(expr) for expr in exprs] return matrix, vec